Two-dimensional one-pulse rotational echo spectra
- Publication type:
- Journal article
- Metadata:
-
- Autoren
- P Blümler
- J Jansen
- B Blümich
- DOI
- 10.1016/0926-2040(94)90044-2
- ISSN
- 0926-2040
- Ausgabe der Veröffentlichung
- 4
- Zeitschrift
- Solid State Nuclear Magnetic Resonance
- Sprache
- en
- Paginierung
- 237 - 240
- Datum der Veröffentlichung
- 1994
- Status
- Published
- Herausgeber
- Elsevier BV
- Herausgeber URL
- http://dx.doi.org/10.1016/0926-2040(94)90044-2
- Datum der Datenerfassung
- 2019
- Titel
- Two-dimensional one-pulse rotational echo spectra
- Ausgabe der Zeitschrift
- 3
Data source: Crossref
- Other metadata sources:
-
- Abstract
- Recently a two-dimensional representation of one-dimensional spinning sideband magic-angle spinning (MAS) spectra has been published with applications to deuteron MAS nuclear magnetic resonance (NMR). The introduction of a new time axis, based on the rotor period, allows the separation of isotropic and anisotropic chemical shifts. It is shown here that, in addition to untangling spinning sideband spectra, data-processing steps can be incorporated which enabled applications of the method to signals from nuclei with anisotropies smaller than those of the quadrupole coupling of deuterons. This is achieved by linear prediction of the rotary echo signals. Advantages and limitations of the algorithm are discussed and demonstrated with experimental results of 13C cross-polarization (CP) MAS spectra of glycine.
- Addresses
- Max-Planck-Institut für Polymerforschung, Mainz, Germany.
- Autoren
- P Blümler
- J Jansen
- B Blümich
- DOI
- 10.1016/0926-2040(94)90044-2
- eISSN
- 1527-3326
- Externe Identifier
- PubMed Identifier: 7834323
- Open access
- false
- ISSN
- 0926-2040
- Ausgabe der Veröffentlichung
- 4
- Zeitschrift
- Solid state nuclear magnetic resonance
- Schlüsselwörter
- Magnetic Resonance Spectroscopy
- Anisotropy
- Algorithms
- Rotation
- Sprache
- eng
- Medium
- Paginierung
- 237 - 240
- Datum der Veröffentlichung
- 1994
- Status
- Published
- Datum der Datenerfassung
- 1994
- Titel
- Two-dimensional one-pulse rotational echo spectra.
- Sub types
- Journal Article
- Ausgabe der Zeitschrift
- 3
Data source: Europe PubMed Central
- Abstract
- Recently a two-dimensional representation of one-dimensional spinning sideband magic-angle spinning (MAS) spectra has been published with applications to deuteron MAS nuclear magnetic resonance (NMR). The introduction of a new time axis, based on the rotor period, allows the separation of isotropic and anisotropic chemical shifts. It is shown here that, in addition to untangling spinning sideband spectra, data-processing steps can be incorporated which enabled applications of the method to signals from nuclei with anisotropies smaller than those of the quadrupole coupling of deuterons. This is achieved by linear prediction of the rotary echo signals. Advantages and limitations of the algorithm are discussed and demonstrated with experimental results of 13C cross-polarization (CP) MAS spectra of glycine.
- Autoren
- P Blümler
- J Jansen
- B Blümich
- Autoren-URL
- https://www.ncbi.nlm.nih.gov/pubmed/7834323
- DOI
- 10.1016/0926-2040(94)90044-2
- ISSN
- 0926-2040
- Ausgabe der Veröffentlichung
- 4
- Zeitschrift
- Solid State Nucl Magn Reson
- Schlüsselwörter
- Algorithms
- Anisotropy
- Magnetic Resonance Spectroscopy
- Rotation
- Sprache
- eng
- Country
- Netherlands
- Paginierung
- 237 - 240
- PII
- 0926-2040(94)90044-2
- Datum der Veröffentlichung
- 1994
- Status
- Published
- Datum, an dem der Datensatz öffentlich gemacht wurde
- 1995
- Titel
- Two-dimensional one-pulse rotational echo spectra.
- Sub types
- Journal Article
- Ausgabe der Zeitschrift
- 3
Data source: PubMed
- Beziehungen:
- Property of