New Calcium Carbonate Nano-particulate Pressed Powder Pellet (NFHS-2-NP) for LA-ICP-OES, LA-(MC)-ICP-MS and μXRF

Publication type:
Journal article
Metadata:
Autoren
  • Wim Boer
  • Simon Nordstad
  • Michael Weber
  • Regina Mertz-Kraus
  • Barbel Hoenisch
  • Jelle Bijma
  • Markus Raitzsch
  • Dorothee Wilhelms-Dick
  • Gavin L Foster
  • Heather Goring-Harford
  • Dirk Nuernberg
  • Folkmar Hauff
  • Henning Kuhnert
  • Federico Lugli
  • Howie Spero
  • Martin Rosner
  • Piet van Gaever
  • Lennart J de Nooijer
  • Gert-Jan Reichart
Autoren-URL
https://www.webofscience.com/api/gateway?GWVersion=2&SrcApp=fis-test-1&SrcAuth=WosAPI&KeyUT=WOS:000800415300001&DestLinkType=FullRecord&DestApp=WOS_CPL
DOI
10.1111/ggr.12425
eISSN
1751-908X
Externe Identifier
  • Clarivate Analytics Document Solution ID: 3U8HG
ISSN
1639-4488
Ausgabe der Veröffentlichung
3
Zeitschrift
GEOSTANDARDS AND GEOANALYTICAL RESEARCH
Schlüsselwörter
  • laser ablation
  • MC-ICP-MS
  • reference materials
  • carbonate
  • homogeneity
  • in situ techniques
Paginierung
411 - 432
Datum der Veröffentlichung
2022
Status
Published
Titel
New Calcium Carbonate Nano-particulate Pressed Powder Pellet (NFHS-2-NP) for LA-ICP-OES, LA-(MC)-ICP-MS and μXRF
Sub types
  • Article
Ausgabe der Zeitschrift
46

Data source: Web of Science (Lite)

Other metadata sources:
Abstract
<jats:p>A new matrix‐matched reference material has been developed – NFHS‐2‐NP (NIOZ Foraminifera House Standard‐2‐Nano‐Pellet) – with element mass fractions, and isotope ratios resembling that of natural foraminiferal calcium carbonate. A 180–355 µm size fraction of planktic foraminifera was milled to nano‐particles and pressed to pellets. We report reference and information values for mass fractions of forty‐six elements measured by six laboratories as well as for <jats:sup>87</jats:sup>Sr/<jats:sup>86</jats:sup>Sr (three laboratories), δ<jats:sup>13</jats:sup>C, δ<jats:sup>18</jats:sup>O (five laboratories) and <jats:sup>206,207,208</jats:sup>Pb/<jats:sup>204</jats:sup>Pb isotope ratios (one laboratory) determined by ICP‐MS, ICP‐OES, MC‐ICP‐MS, isotope ratio mass spectrometry, WD‐XRF and TIMS. Inter‐ and intra‐pellet elemental homogeneity was tested using multiple LA‐ICP‐MS analyses in two laboratories applying spot sizes of 60 and 70 µm. The LA‐ICP‐MS results for most of the elements relevant as proxies for palaeoclimate research show RSD values &lt; 3%, demonstrating a satisfactory homogeneous composition. Homogeneity of <jats:sup>87</jats:sup>Sr/<jats:sup>86</jats:sup>Sr ratios of the pellet was verified by repeated LA‐MC‐ICP‐MS by two laboratories. Information values are reported for Pb isotope ratios and δ<jats:sup>13</jats:sup>C, δ<jats:sup>18</jats:sup>O values. The homogeneity for these isotope systems remains to be tested by LA‐MC‐ICP‐MS and secondary‐ion mass spectrometry. Overall, our results confirm the suitability of NFHS‐2‐NP for calibration or monitoring the quality of <jats:italic>in situ</jats:italic> geochemical techniques.</jats:p>
Autoren
  • Wim Boer
  • Simon Nordstad
  • Michael Weber
  • Regina Mertz‐Kraus
  • Bärbel Hönisch
  • Jelle Bijma
  • Markus Raitzsch
  • Dorothee Wilhelms‐Dick
  • Gavin L Foster
  • Heather Goring‐Harford
  • Dirk Nürnberg
  • Folkmar Hauff
  • Henning Kuhnert
  • Federico Lugli
  • Howie Spero
  • Martin Rosner
  • Piet van Gaever
  • Lennart J de Nooijer
  • Gert‐Jan Reichart
DOI
10.1111/ggr.12425
eISSN
1751-908X
ISSN
1639-4488
Ausgabe der Veröffentlichung
3
Zeitschrift
Geostandards and Geoanalytical Research
Sprache
en
Online publication date
2022
Paginierung
411 - 432
Datum der Veröffentlichung
2022
Status
Published
Herausgeber
Wiley
Herausgeber URL
http://dx.doi.org/10.1111/ggr.12425
Datum der Datenerfassung
2023
Titel
New Calcium Carbonate Nano‐particulate Pressed Powder Pellet (NFHS‐2‐NP) for LA‐ICP‐OES, LA‐(MC)‐ICP‐MS and µXRF
Ausgabe der Zeitschrift
46

Data source: Crossref

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