An effective negative pressure cavitation-microwave assisted extraction for determination of phenolic compounds in P. calliantha H. Andr.
- Publication type:
- Journal article
- Metadata:
-
- Autoren
- Dong-Yang Zhang
- Xiao-Hui Yao
- Ming-Hui Duan
- Meng Luo
- Wei Wang
- Yu-Jie Fu
- Yuan-Gang Zu
- Thomas Efferth
- Autoren-URL
- https://www.webofscience.com/api/gateway?GWVersion=2&SrcApp=fis-test-1&SrcAuth=WosAPI&KeyUT=WOS:000321787600029&DestLinkType=FullRecord&DestApp=WOS_CPL
- DOI
- 10.1039/c3an36534d
- eISSN
- 1364-5528
- Externe Identifier
- Clarivate Analytics Document Solution ID: 183BC
- PubMed Identifier: 23762895
- ISSN
- 0003-2654
- Ausgabe der Veröffentlichung
- 16
- Zeitschrift
- ANALYST
- Paginierung
- 4631 - 4641
- Datum der Veröffentlichung
- 2013
- Status
- Published
- Titel
- An effective negative pressure cavitation-microwave assisted extraction for determination of phenolic compounds in <i>P</i>. <i>calliantha</i> H. Andr.
- Sub types
- Article
- Ausgabe der Zeitschrift
- 138
Data source: Web of Science (Lite)
- Other metadata sources:
-
- Autoren
- Dong-Yang Zhang
- Xiao-Hui Yao
- Ming-Hui Duan
- Meng Luo
- Wei Wang
- Yu-Jie Fu
- Yuan-Gang Zu
- Thomas Efferth
- DOI
- 10.1039/c3an36534d
- eISSN
- 1364-5528
- ISSN
- 0003-2654
- Ausgabe der Veröffentlichung
- 16
- Zeitschrift
- The Analyst
- Sprache
- en
- Paginierung
- 4631 - 4631
- Datum der Veröffentlichung
- 2013
- Status
- Published
- Herausgeber
- Royal Society of Chemistry (RSC)
- Herausgeber URL
- http://dx.doi.org/10.1039/c3an36534d
- Datum der Datenerfassung
- 2024
- Titel
- An effective negative pressure cavitation-microwave assisted extraction for determination of phenolic compounds in P. calliantha H. Andr.
- Ausgabe der Zeitschrift
- 138
Data source: Crossref
- Abstract
- A novel negative pressure and microwave assisted extraction technique (NMAE) was first proposed and applied for extraction of phenolic compounds from pyrola. [C₄MIM]BF₄ aqueous solution was selected as extraction solvent. Optimal extraction conditions were microwave power 700 W, negative pressure -0.07 MPa, temperature 40 °C, liquid-solid ratio 20 : 1, ionic liquid (IL) concentration 0.5 M, extraction time 15 min. The predominance of NMAE was investigated by comparing with microwave-assisted extraction (MAE) and negative pressure cavitation extraction (NPCE) using a first-order kinetics equation. The C∞ values of the target compounds by NMAE were from 0.406 to 5.977 mg g⁻¹ higher than these by MAE and NPCE, which indicated that NMAE had higher extraction yields. The K values of NMAE were also the highest; it was testified that the target compounds could be transferred from matrix into solvent much more effectively by NMAE than by MAE and NPCE. In addition, the NMAE method was validated in terms of repeatability and reproducibility, the relative standard deviation for relative recovery was lower than 5.43 and 8.78%, respectively. Therefore, NMAE was a developed extraction technique for analytical sample preparation. The RP-HPLC-UV method was also successfully applied for the quantification of six target compounds in pyrola.
- Addresses
- State Engineering Laboratory for Bio-Resource Eco-Utilization, PR China.
- Autoren
- Dong-Yang Zhang
- Xiao-Hui Yao
- Ming-Hui Duan
- Meng Luo
- Wei Wang
- Yu-Jie Fu
- Yuan-Gang Zu
- Thomas Efferth
- Thomas Efferth
- DOI
- 10.1039/c3an36534d
- eISSN
- 1364-5528
- Externe Identifier
- PubMed Identifier: 23762895
- Open access
- false
- ISSN
- 0003-2654
- Ausgabe der Veröffentlichung
- 16
- Zeitschrift
- The Analyst
- Schlüsselwörter
- Pyrola
- Phenols
- Plant Extracts
- Chromatography, High Pressure Liquid
- Pressure
- Microwaves
- Liquid-Liquid Extraction
- Sprache
- eng
- Medium
- Print-Electronic
- Online publication date
- 2013
- Paginierung
- 4631 - 4641
- Datum der Veröffentlichung
- 2013
- Status
- Published
- Datum der Datenerfassung
- 2013
- Titel
- An effective negative pressure cavitation-microwave assisted extraction for determination of phenolic compounds in P. calliantha H. Andr.
- Sub types
- Research Support, Non-U.S. Gov't
- Journal Article
- Ausgabe der Zeitschrift
- 138
Data source: Europe PubMed Central
- Abstract
- A novel negative pressure and microwave assisted extraction technique (NMAE) was first proposed and applied for extraction of phenolic compounds from pyrola. [C₄MIM]BF₄ aqueous solution was selected as extraction solvent. Optimal extraction conditions were microwave power 700 W, negative pressure -0.07 MPa, temperature 40 °C, liquid-solid ratio 20 : 1, ionic liquid (IL) concentration 0.5 M, extraction time 15 min. The predominance of NMAE was investigated by comparing with microwave-assisted extraction (MAE) and negative pressure cavitation extraction (NPCE) using a first-order kinetics equation. The C∞ values of the target compounds by NMAE were from 0.406 to 5.977 mg g⁻¹ higher than these by MAE and NPCE, which indicated that NMAE had higher extraction yields. The K values of NMAE were also the highest; it was testified that the target compounds could be transferred from matrix into solvent much more effectively by NMAE than by MAE and NPCE. In addition, the NMAE method was validated in terms of repeatability and reproducibility, the relative standard deviation for relative recovery was lower than 5.43 and 8.78%, respectively. Therefore, NMAE was a developed extraction technique for analytical sample preparation. The RP-HPLC-UV method was also successfully applied for the quantification of six target compounds in pyrola.
- Autoren
- Dong-Yang Zhang
- Xiao-Hui Yao
- Ming-Hui Duan
- Meng Luo
- Wei Wang
- Yu-Jie Fu
- Yuan-Gang Zu
- Thomas Efferth
- Autoren-URL
- https://www.ncbi.nlm.nih.gov/pubmed/23762895
- DOI
- 10.1039/c3an36534d
- eISSN
- 1364-5528
- Ausgabe der Veröffentlichung
- 16
- Zeitschrift
- Analyst
- Schlüsselwörter
- Chromatography, High Pressure Liquid
- Liquid-Liquid Extraction
- Microwaves
- Phenols
- Plant Extracts
- Pressure
- Pyrola
- Sprache
- eng
- Country
- England
- Paginierung
- 4631 - 4641
- Datum der Veröffentlichung
- 2013
- Status
- Published
- Datum, an dem der Datensatz öffentlich gemacht wurde
- 2014
- Titel
- An effective negative pressure cavitation-microwave assisted extraction for determination of phenolic compounds in P. calliantha H. Andr.
- Sub types
- Journal Article
- Research Support, Non-U.S. Gov't
- Ausgabe der Zeitschrift
- 138
Data source: PubMed
- Beziehungen:
- Property of